Comprehensive Method List

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Information about Comprehensive Method List
Health & Medicine

Published on March 12, 2014

Author: KCASBio

Source: slideshare.net

Method List Analyte Matrix LLOQ Units Platform Acebutolol / Diacetolol Human Plasma 5 ng/mL HPLC/UV Acetaminophen (APAP) Human Plasma 0.1 mcg/mL LC-MS/MS Acetaminophen / Tramadol Human Plasma 100 / 5 ng/mL LC-MS/MS Acetylsalicylic Acid / Salicylic Acid Human Plasma 0.25/ 0.75 mcg/mL HPLC/UV Acid Glycoprotein, α1 Human Plasma 3.5 ng/mL ELISA Acyclovir Human Plasma 20 ng/mL HPLC/FL Acyclovir Human Urine 1 mcg/mL HPLC/FL Adipenectin Human Serum 0.8 ng/mL ELISA Alkaline Hematin (see Menstrual Blood) Menstrual Products Allopurinol / Oxypurinol Human Plasma 50 / 100 ng/mL LC-MS/MS Alprazolam Human Plasma 0.5 ng/mL LC-MS/MS Alprazolam / α-Hydroxyalprazolam Dog Plasma 0.5 / 0.5 ng/mL LC-MS/MS Alprazolam / α-Hydroxyalprazolam Human Plasma 0.5 / 0.5 ng/mL LC-MS/MS Aluminum Human Plasma 5 / 2 ng/mL HPLC Aluminum Human Urine 5 / 2 ng/mL HPLC Amikacin Human Serum 0.15 mcg/mL LC-MS/MS Amikacin Human Urine 0.5 mcg/mL LC-MS/MS Aminosalicylic Acid, 5- Human Feces 1 ng on col HPLC/FL Aminosalicylic Acid, 5- Human Urine 2 mcg/mL HPLC/FL Aminosalicylic Acid, 5- Rat Plasma 10 ng/mL LC-MS/MS Aminosalicylic Acid, 5- / N-Acetyl-5-Aminosalicylic Acid Human Plasma 10 / 10 ng/mL HPLC/FL Amiodarone / Desethylamiodarone Human Plasma 10 ng/mL LC-MS/MS Amitriptyline Human Plasma 200 pg/mL LC-MS/MS Amlodipine Human Plasma 50 pg/mL LC-MS/MS Amlodipine Human Plasma 0.15 ng/mL LC-MS/MS Anipamil Human Plasma 5 ng/mL HPLC/FL Aspirin (See Acetylsalicylic Acid) Human Plasma 0.25 ng/mL HPLC/UV Atenolol Human Plasma 10 ng/mL LC-MS/MS Atenolol Human Urine 250 ng/mL LC-MS/MS Atenolol, (R)- and (S)- Human Plasma 20 / 20 ng/mL HPLC/FL Atenolol, (R)- and (S)- Rat Plasma 20 / 20 ng/mL HPLC/FL Atomoxetine Human Plasma 10 ng/mL LC-MS/MS Atorvastatin / p - and o -Hydroxyatorvastatin Human Plasma 0.2 / 0.2 / 0.2 ng/mL LC-MS/MS Azacytidine, 5- Human Plasma 10 ng/mL LC-MS/MS Azithromycin Human Plasma 2 ng/mL LC-MS/MS Benazepril / Benazeprilat Human Plasma 2 / 2 ng/mL LC-MS/MS Benazepril/ Benazeprilat Dog Plasma 0.1 / 0.5 ng/mL LC-MS/MS Bicalutamide Human Plasma 2.5 ng/mL LC-MS/MS Bucladesine Human Plasma 1 ng/mL LC-MS/MS Brompheniramine Human Plasma 0.5 ng/mL LC-MS/MS Brompheniramine / Chlorpheniramine / Pseudeophedrine Human Plasma 0.5 / 0.5 / 5 ng/mL LC-MS/MS Buprenorphine / Norbuprenorphine Dog Plasma 100 pg/mL LC-MS/MS Buprenorphine / Norbuprenorphine Human Plasma 500 pg/mL LC-MS/MS Buprenorphine / Norbuprenorphine Rabbit Plasma 50 pg/mL LC-MS/MS Buspirone / 1-PP Dog Plasma 100 pg/mL LC-MS/MS Fall 2013 KCAS Bioanalytical Services | kcasbio.com | contact us: info@kcasbio.com 1

Method List Analyte Matrix LLOQ Units Platform Buspirone / 1-PP Human Plasma 100 pg/mL LC-MS/MS Butalbital Human Plasma 0.1 mcg/mL HPLC/UV Butorphanol Human Plasma 20 pg/mL LC-MS/MS Caffeine Human Plasma 0.05 mcg/mL HPLC/UV Canrenone Human Plasma 2 ng/mL LC-MS/MS Canrenone Human Urine 20 ng/mL LC-MS/MS Captisol Human Plasma 5 mcg/mL LC-MS/MS Carbamazepine Human Plasma 0.05 mcg/mL HPLC/UV Carisbamate Human Plasma 5 ng/mL LC-MS/MS Cetirizine Human Plasma 2 ng/mL LC-MS/MS Chlorpheniramine Human Plasma 0.5 ng/mL LC-MS/MS Cimetidine Dog Plasma 50 ng/mL HPLC/UV Cimetidine Human Plasma 50 ng/mL HPLC/UV Ciprofloxacin Cat Plasma 25 ng/mL HPLC/FL Ciprofloxacin Human Serum 10 ng/mL LC-MS/MS Cisapride Human Plasma 5 ng/mL HPLC/FL Citric Acid Human Urine 50 mcg/mL LC-MS/MS Clarithromycin Human Plasma 10 ng/mL LC-MS/MS Clonazepam / 7-Hydroxyclonazepam Human Plasma 0.1 / 0.2 pg/mL LC-MS/MS Clotrimazole / Ketoconazole Human Plasma 5 / 50 ng/mL LC-MS/MS Cluster of Differentiation 14 (CD-14) Human Plasma 100 pg/mL ELISA Codeine Human Plasma 1 ng/mL LC-MS/MS Cordycepin Human Plasma 1 ng/mL LC-MS/MS Cortisone Human Plasma 5 ng/mL HPLC/UV Cyclobenzaprine Dog Plasma 0.1 ng/mL LC-MS/MS Cyclobenzaprine Human Plasma 0.2 ng/mL LC-MS/MS Cytarabine (Ara-C) Human Plasma 20 ng/mL LC-MS/MS Deoxycholic Acid Human Plasma 10 ng/mL LC-MS/MS Dexamethasone Human Plasma 0.25 ng/mL LC-MS/MS Dextromethorphan Human Plasma 50 pg/mL LC-MS/MS Dextromethorphan / 3-Hydroxymorphinan / 4-Methoxymorphinan Human Plasma 10 ng/mL HPLC/FL Dextromethorphan / 3-Hydroxymorphinan / 4-Methoxymorphinan Human Urine 0.25 mcg/mL HPLC/FL Dextrorphan Human Plasma 10 ng/mL HPLC/FL Dextrorphan Human Urine 250 ng/mL HPLC/FL Diclofenac Rat Plasma 10 ng/mL HPLC/UV Diclofenac Human Plasma 5 ng/mL LC-MS/MS Digoxin Human Plasma 0.1 ng/mL LC-MS/MS Diltiazem / N-Desmethyldiltiazem / Desacetyldiltiazem Human Plasma 4 / 2 / 1 ng/mL LC-MS/MS Diphenydramine Human Plasma 1 ng/mL LC-MS/MS Dipyridamole Human Plasma 50 ng/mL LC-MS/MS DNA Quantitation Human Tissue 50 ng/mL Fluorometric Doxepin / Nordoxepin Human Urine 0.25 / 0.20 ng/mL LC-MS/MS Doxorubicin Human Plasma 100 ng/mL LC-MS/MS Doxorubicin Human Urine 1.5 ng/mL LC-MS/MS Fall 2013 KCAS Bioanalytical Services | kcasbio.com | contact us: info@kcasbio.com 2

Method List Analyte Matrix LLOQ Units Platform Doxorubicin/Doxorubicinol Human Plasma 0.5 / 0.5 ng/mL LC-MS/MS Doxylamine Human Plasma 5 / 100 ng/mL HPLC/UV Doxylamine Human Urine 5 / 100 ng/mL HPLC/UV Dyclonine Dog Serum 1 ng/mL LC-MS/MS Ebastine Human Plasma 10 ng/mL HPLC/UV Efavirenz Human Plasma 50 ng/mL LC-MS/MS Enalapril & Enalaprilat Human Plasma 0.25 ng/mL LC-MS/MS Esomeprazole Human Plasma 0.25 ng/mL LC-MS/MS Ethambutol Human DBS 100 ng/mL LC-MS/MS Famotidine Human Plasma 2 ng/mL LC-MS/MS Famotidine Human Urine 2 ng/mL LC-MS/MS Felodipine Human Plasma 25 pg/mL LC-MS/MS Femoxitine / N-Desmethylfemoxitine Human Plasma 5 ng/mL HPLC/FL Femoxitine / N-Desmethylfemoxitine Monkey Plasma 5 ng/mL HPLC/FL Fenofibric Acid Human Plasma 20 ng/mL LC-MS/MS Fexofenadine Human Plasma 1 ng/mL LC-MS/MS Fexofenadine Mouse Plasma 25 ng/mL LC-MS/MS Fexofenadine Rabbit Plasma 25 ng/mL LC-MS/MS Fexofenadine Rat Plasma 25 ng/mL LC-MS/MS Flavoxate / MFCA metabolite Human Plasma 0.1 ng/mL LC-MS/MS Flurbiprofen Human Plasma 5 ng/mL LC-MS/MS Flurbiprofen, (R)- and (S)- Human Plasma 0.25 mcg/mL HPLC/FL Flurbiprofen, (R)- and (S)- Human Urine 0.5 mcg/mL HPLC/FL Furosemide Human Plasma 50 ng/mL LC-MS/MS Furosemide Human Urine 50 ng/mL LC-MS/MS Gemcitabine Human Plasma 40 ng/mL HPLC/UV Gemcitabine Human Urine 40 ng/mL HPLC/UV Gemfibrozil Human Plasma 0.5 mcg/mL HPLC/UV Ghrelin Active Human Plasma 100 pg/mL ELISA Ghrelin Total Human Plasma 200 pg/mL ELISA Gliclazide Human Plasma 100 ng/mL HPLC/UV Granisetron Dog Plasma 0.1 ng/mL LC-MS/MS Guaifenesin Human Plasma 5 ng/mL LC-MS/MS Guaifenesin / Naproxen Human Plasma 10 / 250 ng/mL LC-MS/MS Haloperidol Human Plasma 25 pg/mL LC-MS/MS Hepatocyte Growth Factor (HGF) Human Plasma 400 pg/mL ELISA Heptazyme Antibodies Monkey Serum 1:25,600 titer ELISA Homocysteine Dog Plasma 5 mcg/mL LC-MS/MS Homocysteine Rat Plasma 5 mcg/mL LC-MS/MS Hydrochlorothiazide (HCTZ) Human Plasma 1 ng/mL HPLC/UV Hydrochlorothiazide (HCTZ) Human Urine 0.05 mcg/mL HPLC/UV Hydrocodone Human Plasma 0.1 ng/mL LC-MS/MS Hydromorphone Dog Plasma 20 pg/mL LC-MS/MS Hydromorphone Human Plasma 40 pg/mL LC-MS/MS Hydroxymephenytoin, (R)-4- / Hydroxymephenytoin, (S)-4- Human Plasma 10 ng/mL LC-MS/MS Fall 2013 KCAS Bioanalytical Services | kcasbio.com | contact us: info@kcasbio.com 3

Method List Analyte Matrix LLOQ Units Platform Hydroxymephenytoin, (R)-4- / Hydroxymephenytoin, (S)-4- Human Saliva 10 ng/mL LC-MS/MS Hydroxymephenytoin, (R)-4- / Hydroxymephenytoin, (S)-4- Human Urine 0.1 mcg/mL LC-MS/MS Hydroxymidazolam, a- / Hydoxymidazolam, 4- Dog Plasma 2 / 2 ng/mL LC-MS/MS Hydroxymidazolam, a- / Hydoxymidazolam, 4- Rat Plasma 2 / 2 ng/mL LC-MS/MS Ibuprofen Human Plasma 0.25 mcg/mL LC-MS/MS Ibuprofen, (R)- and (S)- Human Plasma 0.25 mcg/mL HPLC/UV Ibuprofen, (R)- and (S)- Human Urine 2.5 mcg/mL HPLC/FL Imipramine / Desipramine Human Plasma 0.1 ng/mL LC-MS/MS Indocyanine Green (ICG) Human Plasma 0.3 mcg/mL HPLC/UV Indomethacin Human Plasma 10 ng/mL LC-MS/MS Indomethacin Plasma/Serum 20 ng/mL HPLC/FL Interferon alpha Human Serum 10 pg/mL ELISA Isotretinoin / 4-Oxo-Isotretinoin Human Plasma 10 ng/mL LC-MS/MS Isradapine Human Plasma 0.1 ng/mL LC-MS/MS Ketoconazole Human Plasma 50 ng/mL HPLC/FL Ketoconazole / Clotrimazole Human Plasma 50 / 5 ng/mL LC-MS/MS Ketoprofen Human Plasma 0.25 ng/mL LC-MS/MS Lansoprazole Human Plasma 0.25 ng/mL LC-MS/MS Levofloxacin Rabbit Plasma 10 ng/mL LC-MS/MS Lorazepam Human Plasma 1 ng/mL LC-MS/MS Losartan / Carboxylosartan Human Plasma 2 / 2 ng/mL LC-MS/MS Meloxicam Human Plasma 10 ng/mL LC-MS/MS Melphalan Human Plasma 25 ng/mL LC-MS/MS Memantine Human Plasma 0.5 ng/mL LC-MS/MS Memantine N-Glucuronide Human Plasma 0.2 ng/mL LC-MS/MS Menstrual Blood (as Alkaline Hematin) Menstrual Products 1 mL Colorimetric Monocyte Chemotatic Protein 1 (MCP-1) Human Plasma 30 pg/mL ELISA Monocyte Chemotatic Protein 3 (MCP-3) Human Plasma 15 pg/mL ELISA Mephenytoin, (R)- / Mephenytoin, (S)- Human Plasma 10 ng/mL LC-MS/MS Mephenytoin, (R)- / Mephenytoin, (S)- Human Saliva 10 ng/mL LC-MS/MS Mephenytoin, (R)- / Mephenytoin, (S)- Human Urine 0.1 mcg/mL LC-MS/MS Mercaptopurine, 6- / 6-Thiouric Acid Human Plasma 2 / 20 ng/mL LC-MS/MS Mercaptopurine, 6- / 6-Thiouric Acid Human Urine 6 / 60 ng/mL LC-MS/MS Metformin Human Plasma 20 ng/mL LC-MS/MS Methocarbamol Human Plasma 0.1 mcg/mL HPLC/FL Methylnicotinamide Human Plasma 10 ng/mL LC-MS/MS Methylphenidate Human Plasma 0.1 ng/mL LC-MS/MS Methylprednisolone Human Plasma 2.5 ng/mL LC-MS/MS Metoclopramide Human Plasma 1 ng/mL HPLC/UV Metoclopramide Human Urine 60 ng/mL HPLC/FL Metoprolol Human Plasma 1 ng/mL LC-MS/MS Metoprolol / Hydroxymetoprolol Human Plasma 2.5 ng/mL HPLC/FL Metoprolol / Hydroxymetoprolol Human Urine 1000 ng/mL HPLC/FL Midazolam / α-Hydroxymidazolam Human Plasma 0.5 / 0.5 ng/mL LC-MS/MS Midazolam / 1-Hydroxymidazolam / 4-Hydroxymidazolam Human Urine 10 / 2 / 2 ng/mL LC-MS/MS Fall 2013 KCAS Bioanalytical Services | kcasbio.com | contact us: info@kcasbio.com 4

Method List Analyte Matrix LLOQ Units Platform Midazolam / α-Hydroxymidazolam Human Urine 20 / 0.5 ng/mL LC-MS/MS Molindone Human Plasma 0.25 ng/mL LC-MS/MS Monocyte Chemotactic Protein 1 (MCP-1) Human Plasma 30 pg/mL ELISA Monocyte Chemotactic Protein 3 (MCP-3) Human Plasma 15 pg/mL ELISA Morphine / Morphine-3-Glucuronide / Morphine-6-Glucuronide Dog Plasma 0.5 / 5 / 2 ng/mL LC-MS/MS Morphine / Morphine-3-Glucuronide / Morphine-6-Glucuronide Human Plasma 0.5 / 5 / 2 ng/mL LC-MS/MS Morphine / Morphine-3-Glucuronide / Morphine-6-Glucuronide Ovine Plasma 0.5 / 5 / 2 ng/mL LC-MS/MS Moxifloxacin Human DBS 100 ng/mL LC-MS/MS Moxifloxacin Human Plasma 20 ng/mL LC-MS/MS Naproxen Human Plasma 0.25 mcg/mL LC-MS/MS Niacin (Nicotinic Acid) / Nicotinuric Acid Human Urine 25 ng/mL LC-MS/MS Nifedipine / NPO Human Plasma 1 ng/mL LC-MS/MS Nitrofurantoin Human Plasma 5 ng/mL HPLC/UV Nitrofurantoin Human Urine 2 mcg/mL HPLC/UV Noroxycodone Human Plasma 0.25 ng/mL LC-MS/MS Olanzapine Human Plasma 0.1 ng/mL LC-MS/MS Omeprazole Human Plasma 5 ng/mL LC-MS/MS Ondansetron Human Plasma 0.5 ng/mL LC-MS/MS Oxandrolone Human Plasma 0.25 ng/mL LC-MS/MS Oxaprozin Human Plasma 2 mcg/mL HPLC/UV Oxybutynin / N-Desethyloxybutynin Human Plasma 50 / 250 pg/mL LC-MS/MS Oxycodone / Noroxycodcone / Oxymorphone Human Plasma 0.25 ng/mL LC-MS/MS Oxymorphone Human Plasma 0.25 ng/mL LC-MS/MS Paclitaxel Human Plasma 100 pg/mL LC-MS/MS Paclitaxel Human Plasma 1 ng/mL LC-MS/MS Paclitaxel Human Urine 5 ng/mL LC-MS/MS Pantoprazole Human Plasma 10 ng/mL LC-MS/MS Paraxanthine Human Plasma 25 ng/mL HPLC/UV Paroxetine Human Plasma 0.2 ng/mL LC-MS/MS Pentazocine Human Plasma 1 ng/mL LC-MS/MS Phenylephrine Human Plasma 0.5 ng/mL LC-MS/MS Phenylephrine Human Urine 5 ng/mL LC-MS/MS Phenytoin Human Plasma 0.25 mcg/mL HPLC/UV Phenytoin Human Urine 1 mcg/mL HPLC/UV Phenytoin / Phenylhydantoin / Phenobarbitol (Free Assay) Human Urine 0.1 mcg/mL HPLC/UV Pindolol Human Plasma 1 ng/mL HPLC/UV Piroxicam Human Plasma 50 ng/mL HPLC/UV Potassium Human Urine 8 mM ICP-MS Prednisolone Human Plasma 1 ng/mL HPLC/UV Prednisone Human Plasma 1 ng/mL HPLC/UV Primidone Human Plasma 25 ng/mL LC-MS/MS Propafenone / N-Despropylpropafenone- / 5-Hydroxypropafenone Human Plasma 250 pg/mL LC-MS/MS Fall 2013 KCAS Bioanalytical Services | kcasbio.com | contact us: info@kcasbio.com 5

Method List Analyte Matrix LLOQ Units Platform Propofol Human Plasma 2.5 ng/mL HPLC/FL Propoxyphene/Norpropoxyphene Human Plasma 1 ng/mL LC-MS/MS Propranolol / 4-Hydroxypropranolol Human Plasma 2.5 ng/mL HPLC/FL Propranolol Glucuronide Human Urine 1 mcg/mL HPLC/FL Pseudoephedrine Human Plasma 5 ng/mL LC-MS/MS Pyrazinamide Human DBS 10 mcg/mL LC-MS/MS Quinidine Human Plasma 10 ng/mL HPLC/UV Ranitidine Human Plasma 5 ng/mL HPLC/UV Reserpine Human Plasma 25 pg/mL HPLC/FL Resistin Human Plasma 160 ng/mL ELISA Ribavirin Human Plasma 5 ng/mL LC-MS/MS Rifampin Human DBS 200 ng/mL LC-MS/MS Risperidone Human Plasma 0.1 ng/mL LC-MS/MS Ropinirole Human Plasma 20 pg/mL LC-MS/MS Ropinirole Mini-Pig Plasma 20 pg/mL LC-MS/MS Rosuvastatin Human Plasma 0.2 ng/mL LC-MS/MS Salicylic Acid Plasma 0.7 mcg/mL HPLC/FL Salicylic Acid Urine 9.2 mcg/mL HPLC/FL Salicyluric Acid Human Plasma 25 ng/mL HPLC/UV Salicyluric Acid Human Urine 2.5 mcg/mL HPLC/UV Simvastatin / Simvastatin Hydroxy Acid Human Plasma 50 / 50 pg/mL LC-MS/MS Spironolactone Human Plasma 0.5 ng/mL LC-MS/MS Sumatriptan Human Plasma 0.5 ng/mL LC-MS/MS Tacrolimus Rat DBS 5 ng/mL LC-MS/MS Tacrolimus Dog Whole Blood 0.1 ng/mL LC-MS/MS Tacrolimus Human Whole Blood 0.5 ng/mL LC-MS/MS Temazepam Human Plasma 20 ng/mL LC-MS/MS Tenofovir Human Plasma 10 ng/mL LC-MS/MS Tenoxicam Human Plasma 20 ng/mL HPLC/UV Terbinafine Human Nail 5 pg/mg LC-MS/MS Terbinafine / N-Desmethylterbinafine Human Plasma 40 pg/mL LC-MS/MS Testosterone (total) Human Serum 5 ng/dL RIA Theophylline Human Plasma 50 ng/mL HPLC/UV Theophylline Human Plasma 0.2 mcg/mL HPLC/UV Theophylline Human Serum 0.2 mcg/mL HPLC/UV Tizanidine Human Plasma 100 pg/mL LC-MS/MS Tolbutamide / Carboxytolbutamide / Hydroxytolbutamide Human Plasma 0.25 / 0.5 / 0.5 mcg/mL HPLC/UV Tolbutamide / Carboxytolbutamide / Hydroxytolbutamide Human Urine 0.25 / 0.5 / 0.5 mcg/mL HPLC/UV Tramadol Dog Plasma 2 ng/mL LC-MS/MS Tramadol / Acetaminophen Human Plasma 2.5 / 100 ng/mL LC-MS/MS Tretinoin Human Plasma 1 ng/mL LC-MS/MS Tretinoin / Isotretinoin Human Plasma 10 / 10 ng/mL LC-MS/MS Triamcinolone Human Plasma 20 pg/mL LC-MS/MS Triamterene Human Plasma 2 ng/mL LC-MS/MS Fall 2013 KCAS Bioanalytical Services | kcasbio.com | contact us: info@kcasbio.com 6

Method List Analyte Matrix LLOQ Units Platform Tyramine Human Plasma 1 ng/mL LC-MS/MS Valproic Acid Human Plasma 0.5 mcg/mL LC-MS/MS Valproic Acid Human Plasma 4 mcg/mL LC-MS/MS Venlafaxine / O-Desmethylvenlafaxine Human Plasma 2.5 ng/mL LC-MS/MS Vitamin B6 Human Plasma 50 ng/mL LC-MS/MS Vitamin E Human Plasma 0.5 mcg/mL HPLC/UV Warfarin, (R)- and (S)- Human Plasma 50 ng/mL HPLC/FL Xanthine Human Urine 1 mcg/mL HPLC/UV Xanthine Human Plasma 0.5 mcg/mL HPLC/UV Zolpidem Human Plasma 0.5 ng/mL LC-MS/MS Zonisamide Human Serum 50 ng/mL HPLC/UV Fall 2013 KCAS Bioanalytical Services | kcasbio.com | contact us: info@kcasbio.com 7

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